I-Anhui Rencheng Technology Co., Ltd.

Cannabinoids Stimulants CAS: 28578-16-7 Ethyl Glycidate Pmk Oli

Inkcazelo emfutshane:

Qhagamshelana nam: Anhui Rencheng Technology Co., Ltd.
WhatsApp/Wechat/Telegram: +8615656977652
Wickr Me:weichengju
Email:002@ahrencheng.com

Igama leMveliso: PMK ethyl glycidate
CAS: 28578-16-7
Ifomula yemolekyuli:C13H14O5
Ubunzima beMolekyuli: 227.1


Iinkcukacha zeMveliso

Iithegi zeMveliso

Ulwazi olusisiseko

Igama lemveliso

I-2-Bromo-4'-methylpropiophenone

CAS

1451-82-7

EINECS

696-162-0

Ifomula yemolekyuli

I-C10H11BrO

Ubunzima beMolekyuli

227.1

Indawo yokubilisa

75-77ºC

Indawo yokuflasha

59°C

Imbonakalo

Umgubo omhlophe wekristale

PSA

17.07000

LogP

3.00

Iimeko zokugcina

Isikhenkcisi

Izinto eziphathekayo

Umsebenzi weMichiza yeMveliso / i-Organic Intermediates

Umsebenzi

Ikakhulu isetyenziswa kwi-Pharmaceutical Intermediates / intermediate medical

I-1) Ngaphantsi kokhuseleko lwe-argon, yongeza (4g, 30mmol) ye-anhydrous aluminium chloride kwi-flask yokusabela, uze ungeze i-20ml ye-anhydrous dichloromethane, kwaye ugxobhoze ukuchithwa.Emva kokuchithwa, yongeza (1.7g, 10mmol) i-2-bromopropionyl chloride, kwaye uqhubeke uvuselela i-20 min.Emva koko (0.92g, 10mmol) i-toluene yongezwa, kwaye ukudibanisa kwagqitywa nge-dropwise kwimizuzu engama-30.Emva kokuba udibaniso lwe-dropwise lugqityiwe, i-reflux ye-2H, kwaye ipholile kwiqondo lokushisa emva kokuba i-reflux igqityiwe.

2) Emva kokupholisa, uthele isisombululo kwi-40ml yamanzi e-ice, yongeza i-20ml ye-dichloromethane kunye ne-20ml ye-6N i-hydrochloric acid, xubha ngamandla kwaye uze ume kwaye uhlukane kwiindidi.Emva kokubekwa, isigaba se-dichloromethane somgangatho osezantsi sashiywa.Emva kokuhlamba isigaba se-dichloromethane nge-1NHCL kabini, yomiswa nge-anhydrous magnesium sulfate, yahluzwa, kunye ne-rotary evaporated ukuze kufumaneke into e-oyile ebonakalayo.

3) Beka into ebonakalayo kwisitya secrystallization kwaye wongeze i-ether ukunyibilika, emva koko udibanise i-ether ye-petroleum de ibe yi-turbid kancinane, gubungela kwaye udibanise iqhekeza lephepha ukuze ume ngxi kwi-fume hood ukuze udibanise ukufumana i-1.37g yemveliso ye-2-bromo. -4' -Iikristale ezicacileyo ze-methyl phenylacetone.

I-Pharmaceutical-Chemical-CAS-1451-82-7-in-Stock-with-Top-Quality-(4)

Usetyenziso

I-2-Bromo-4'-methylpropiophenone ingasetyenziselwa njengendawo ephakathi kwi-pharmaceutical synthesis.Njengokulungiswa kwe-4-methylmethcathinone (4-MMC), eyaziwa ngokuba yiMephedrone (Mephedrone), amanye amagama aquka i-2-Bromo-1- (p-tolyl) ipropan-1-enye, i-2-Bromo-4'-methylpropiophenone , EY1&VR D1 okanye CAS 1451-82-7.

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